HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 24899957, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Valeryl chloride | HCID 61186 | — |
| Reactant | 7,8,9,10-tetrahydro-6H-benzo[b]-cyclohepta[d]furan-2-ylamine | HCID 12884883 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 24899957 | HCID 24899957 | 49.6% |
Reaction Steps
Following the procedure of Example 1, 7,8,9,10-tetrahydro-6H-benzo[b]-cyclohepta[d]furan-2-ylamine (0.25 g, 1.2 mmol), valeryl chloride (0.16 mL, 1.4 mmol), and pyridine (0.30 mL, 3.7 mmol) in acetonitrile (15 mL) provided N-(7,8,9,10-tetrahydro-6H-benzo[b]cyclohepta[d]furan-2-yl)pentanamide (0.17 g). MS (ESI) m/z 286([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601856B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-f3524516097749c782fe1654209659c0 |
| Source note | uspto-grants-2009_10 |