HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylbenzoyl chloride → HCID 24897431, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylbenzoyl chloride | HCID 74375 | — |
| Reactant | HCID 57890287 | HCID 57890287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 24897431 | HCID 24897431 | 81.4% |
Reaction Steps
Following the procedure of Example 1, 6,7,8,9,10,11-Hexahydro-benzo[b]-cycloocta[d]furan-2-ylamine (0.15 g, 0.70 mmol), m-toluoyl chloride (0.096 mL, 0.73 mmol), and poly(vinylpyridine) (0.5 g) in dichloromethane (17 mL) provided N-(6,7,8,9,10,11-hexahydrobenzo[b]cycloocta[d]furan-2-yl)-3-methylbenzamide (0.19 g). MS (ESI) m/z 334 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601856B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-fb125fd208c148549b93030e67df2360 |
| Source note | uspto-grants-2009_10 |