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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1819908Generated: October 31, 2026

Benzenepropanoyl chloride → HCID 24897635, compound

https://huagongshe.com/reaction/1819908

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzenepropanoyl chlorideHCID 64801—
ReactantHCID 57890287HCID 57890287—
Solvent1,1-DichloroethaneHCID 6365—
ProductHCID 24897635HCID 2489763570.9%

Reaction Steps

Following the procedure of Example 1, 6,7,8,9,10,11-Hexahydro-benzo[b]-cycloocta[d]furan-2-ylamine (0.15 g, 0.69 mmol), hydrocinnamoyl chloride (0.10 mL, 0.69 mmol), and poly(vinylpyridine) (0.5 g) in dichloroethane (8 mL) provided N-(6,7,8,9,10,11-hexahydrobenzo[b]cycloocta[d]furan-2-yl)-3-phenylpropanamide (0.17 g). MS (ESI) m/z 348 ([M+H]+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07601856B2
Source datasetuspto-grants-2009_10
ORD IDord-fd937896f5da4642b7a19a6672e456a8
Source noteuspto-grants-2009_10