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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1819986Generated: October 25, 2026

Succinic acid bis(3,4-dibenzyloxybenzylamide) → HCID 10383893, compound

https://huagongshe.com/reaction/1819986

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSuccinic acid bis(3,4-dibenzyloxybenzylamide)HCID 57634450—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventTetrahydrofuranHCID 8028—
ProductHCID 10383893HCID 10383893—

Reaction Steps

Succinic acid bis(3,4-dibenzyloxybenzylamide) (300 mg, 0.42 mmol) was dissolved in THF (50 ml) in a pressure bottle and warmed to 35 C to ensure dissolution of the solid. Palladium on carbon (50 mg 10% Pd/C) was added, and the vessel was pressurized with hydrogen (to 3 atm). The reaction was agitated for 1 hour at room temperature, whereupon TLC revealed reaction had gone to completion. The catalyst was removed by

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07601876B2
Source datasetuspto-grants-2009_10
ORD IDord-7de437814d16454d96591a2737cb488f
Source noteuspto-grants-2009_10