HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic acid bis(3,4-dibenzyloxybenzylamide) → HCID 10383893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic acid bis(3,4-dibenzyloxybenzylamide) | HCID 57634450 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 10383893 | HCID 10383893 | — |
Reaction Steps
Succinic acid bis(3,4-dibenzyloxybenzylamide) (300 mg, 0.42 mmol) was dissolved in THF (50 ml) in a pressure bottle and warmed to 35 C to ensure dissolution of the solid. Palladium on carbon (50 mg 10% Pd/C) was added, and the vessel was pressurized with hydrogen (to 3 atm). The reaction was agitated for 1 hour at room temperature, whereupon TLC revealed reaction had gone to completion. The catalyst was removed by
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601876B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-7de437814d16454d96591a2737cb488f |
| Source note | uspto-grants-2009_10 |