HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1820136Generated: October 30, 2026
Heptanoyl chloride → HCID 11688185, compound
https://huagongshe.com/reaction/1820136
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Heptanoyl chloride | HCID 17313 | — |
| Reactant | 4-Bromo-2,6-xylidine | HCID 90549 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11688185 | HCID 11688185 | 33% |
Reaction Steps
Heptanoyl chloride (16 mg) was added to 4-bromo-2,6-dimethyl-aniline (20 mg) dissolved in acetonitrile and heated to 70° C. for 16 hours. The reaction mixture was concentrated in vacuo, redissolved in dimethyl sulfoxide/methanol (1:1, 0.5 mL) and subjected to preparative LC-MS purification to furnish 10 mg (33% yield) of the title compound as an oil. LC-MS (m/z) 313 (MH+); tR=3.33, (UV, ELSD) 93%, 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07601870B2 |
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| Source dataset | uspto-grants-2009_10 |
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| ORD ID | ord-ddc3d0ad6c3443e2a2c1a6f9fb0f2b47 |
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| Source note | uspto-grants-2009_10 |
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