HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluoro-4-hydroxybenzaldehyde → HCID 10813662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluoro-4-hydroxybenzaldehyde | HCID 587250 | — |
| Reactant | HCID 10916287 | HCID 10916287 | — |
| Product | HCID 10813662 | HCID 10813662 | 81.3% |
Reaction Steps
14.2 g (35.8 mmol) of (2S,3S,4S,5R,6S)-3,4,5-triacetoxy-6-bromo-tetrahydro-pyran-2-carboxylic acid methyl ester is reacted analogously to Example LE1a with 5.05 g of 3-fluoro-4-hydroxybenzaldehyde, and after working-up and purification, 13.3 g (29.1 mmol, 81%) of the title compound is isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07605136B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-58b3f907e61b4944a4f8a78333470cb8 |
| Source note | uspto-grants-2009_10 |