HCID 87964453, compound → HCID 69726227, compound

HRID 1820685Notes

Reaction equation

HRID 1820685 reaction equation
C(OC([NH:8][C@H:9]([C:14]([NH:16][CH:17]([C:26]#[N:27])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=1[O:24][CH3:25])=[O:15])[CH2:10][CH:11]([CH3:13])[CH3:12])=O)(C)(C)C>C(O)=O>[C:26]([CH:17]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=1[O:24][CH3:25])[NH:16][C:14](=[O:15])[C@H:9]([CH2:10][CH:11]([CH3:13])[CH3:12])[NH2:8])#[N:27]

Participants

3

Reactant 1

HCID 87964453HCID 87964453, compound

Product 1

HCID 69726227HCID 69726227, compoundYield 99.5%

Reagents, catalysts & solvents 1

HCID 284Formic AcidSolvent

Procedure

The product from step (i) (3.70 g) in formic acid (40 ml) was stirred for 90 min at room temperature then the solvent was removed under vacuum to give a yellow oil (2.7 g).

Workup

  1. customthe solvent was removed under vacuum

Sources & evidence

ORD record
ord-4ede8fc05de94c118ace3bed75d177d5
Source dataset
uspto-grants-2009_10
Patent number
US07605159B2

Reaction notes

Loading…