HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Dimethylcarbamoyloxy-5-methanesulfonyl-benzoic acid benzyl ester → 2-Dimethylcarbamoyloxy-5-methanesulfonyl-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Dimethylcarbamoyloxy-5-methanesulfonyl-benzoic acid benzyl ester | HCID 69036075 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Dimethylcarbamoyloxy-5-methanesulfonyl-benzoic acid | HCID 69039101 | — |
Reaction Steps
1 mmol of 2-dimethylcarbamoyloxy-5-methanesulfonyl-benzoic acid benzyl ester was dissolved in 5 ml of methanol. 25 mg of palladium 10% on charcoal was added and the reaction mixture hydrogenated at room temperature to yield the title compound as a slightly yellowish solid. MS (m/e): 288.0 (MH+, 66%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07605163B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-df9be6c344f14cd7ab0762dfdd8e9d11 |
| Source note | uspto-grants-2009_10 |