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1-[2-Fluoro-4-(methylsulfonyl)phenyl]piperazine → (2-Benzyloxy-5-methanesulfonyl-phenyl)-[4-(2-fluoro-4-methanesulfonyl-phenyl)-piperazin-1-yl]-methanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-[2-Fluoro-4-(methylsulfonyl)phenyl]piperazine | HCID 2782730 | — |
| 反応物 | 2-Benzyloxy-5-methanesulfonyl-benzoic acid | HCID 68826683 | — |
| 生成物 | (2-Benzyloxy-5-methanesulfonyl-phenyl)-[4-(2-fluoro-4-methanesulfonyl-phenyl)-piperazin-1-yl]-methanone | HCID 69037318 | — |
反応手順
The title compound was prepared in analogy to example 5 from 1-(2-Fluoro-4-methanesulfonyl-phenyl)-piperazine (commercial) and 2-Benzyloxy-5-methanesulfonyl-benzoic acid (compound 7.5). MS (m/e): 547.4 (MH+, 100%)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07605163B2 |
| 出典データセット | uspto-grants-2009_10 |
| ORD ID | ord-70e23f77577440fe9a44e3ce3bd58b68 |
| 出典メモ | uspto-grants-2009_10 |