HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → (2-Chloro-4-nitrophenyl)acetic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(2-Chloro-4-nitrophenyl)acetic acid | HCID 12510588 | — |
| Product | (2-Chloro-4-nitrophenyl)acetic acid chloride | HCID 85969188 | — |
Reaction Steps
8.10 g (37.6 mmol) of (2-chloro-4-nitrophenyl)acetic acid is suspended in 40 mL of thionyl chloride and refluxed for 2 hours. The product is reacted further without any more purification. Crude yield: 8.80 g (100% of theory); C8H5Cl2NO3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07605176B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-f53f9df26c0e40d9aa4c01bfc8cfba10 |
| Source note | uspto-grants-2009_10 |