HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → 1H-Pyrrolo[2,3-b]pyridine, 5-(3,4-dimethoxyphenyl)-1-(phenylsulfonyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | 5-(3,4-Dimethoxy-phenyl)-1H-pyrrolo[2,3-b]pyridine | HCID 10149230 | — |
| Product | 1H-Pyrrolo[2,3-b]pyridine, 5-(3,4-dimethoxyphenyl)-1-(phenylsulfonyl)- | HCID 57891693 | — |
Reaction Steps
1-Benzenesulfonyl-5-(3,4-dimethoxy-phenyl)-1H-pyrrolo[2,3-b]pyridine 132 was prepared using the same protocol as described in Example 9, substituting 3-(3,4-Dimethoxy-phenyl)-1H-pyrrolo-[2,3-b]pyridine and quioline-8-sulfonyl chloride with 5-(3,4-Dimethoxy-phenyl)-1H-pyrrolo-[2,3-b]pyridine and benzene sulfonyl chloride respectively. MS(ESI) [M+H+]+=395.20
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07605168B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-6b7424d54e054b72930b6f7ed722d54a |
| Source note | uspto-grants-2009_10 |