Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1821062Generated: November 1, 2026

Dimethyldioxirane → 5,7-Bis-(benzyloxy)-2-(4-(benzyloxy)phenyl)-3-hydroxy-4H-chromen-4-one

https://huagongshe.com/reaction/1821062

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyldioxiraneHCID 115197—
ReactantMLS000517991HCID 11180247—
SolventAcetoneHCID 180—
SolventDichloromethaneHCID 6344—
Product5,7-Bis-(benzyloxy)-2-(4-(benzyloxy)phenyl)-3-hydroxy-4H-chromen-4-oneHCID 11272906—

Reaction Conditions

Temperature0 °C

Reaction Steps

To a solution containing 1.00 g (1.85 mmol) of 3 in 30 mL of CH2Cl2 at 0° C. was added 30 mL of a 0.9-0.11 M solution of DMDO in acetone. The reaction mixture was stirred at 0° C. overnight under N2.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07605241B2
Source datasetuspto-grants-2009_10
ORD IDord-28f49aa3149243459ef6157db69de254
Source noteuspto-grants-2009_10