HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formate → HCID 178425605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formate | HCID 283 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-(3-Methylphenylaminocarbonylamino)eth-1-ylamine | HCID 22138859 | — |
| Reactant | HCID 178467516 | HCID 178467516 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178425605 | HCID 178425605 | — |
Reaction Steps
To a solution of N-(4-ethoxy-1,1-dioxo-1,2,5-thiadiazol-3-yl)-L-tyrosine tert-butyl ester from Step A (150 mg, 0.38 mmol) and the formate salt of 2-(3-methylphenylaminocarbonylamino)eth-1-ylamine from Step B (210 mg, 0.89 mmol) in ethanol (10 mL) was added triethylamine (133 mg, 1.44 mmol). The reaction was stirred at room temperature overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07605166B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-5377751a3e52402791cf5d097f6d290c |
| Source note | uspto-grants-2009_10 |