Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178424441 | HCID 178424441 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23677956 | HCID 23677956 | 100.3% |
Reaction Steps
0.18 mL (0.36 mmol) of 2 mol/L aqueous sodium hydroxide solution was added to an ethanol (2 mL) solution containing 100 mg (0.361 mmol) of 6-chloro-3-(2-cyclopropyl-6-methylphenoxy)-4-pyridazinol, and the resulting mixture was stirred at 50° C. for 4 hours. The reaction mixture was concentrated to obtain 108 mg (0.361 mmol, Yield: 100%) of sodium 6-chloro-3-(2-cyclopropyl-6-methylphenoxy)-4-pyridazinolate (Compound No. 3805).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07608563B2 |
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| Source dataset | uspto-grants-2009_10 |
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| ORD ID | ord-6d6b88c626e7480ba4b2abc5be356bb0 |
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| Source note | uspto-grants-2009_10 |
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