HCID 57893484, compound → HCID 11042299, compound

Participants

Reaction Steps

Phenyl(1H-pyrrolo[2,3-c]pyridin-3-yl)methanone (379 mg, 78%) was prepared using phenyl(1H-pyrrolo[2,3-c]pyridin-3-yl)methanol (Example 97) as a yellow solid following the procedure described for Reference Example 13: Rf 0.48 (90:10 methylene chloride/methanol); mp 218-220° C.; 1H NMR (300 MHz, DMSO-d6) δ7.55-7.58 (2H, m), 7.62-7.65 (1H, m), 7.81-7.83 (2H, m), 8.09-8.10 (1H, d, J=5.4 Hz), 8.19 (1H, s), 8.33-8.34 (1H, d, J=5.4 Hz), 8.88 (1H, s), 12.50 (1H, br s); ESI MS m/z 223 [C14H10N2O+H]+; HPLC (Method A) 96.6% (AUC), tR=13.2 min.

Provenance & Evidence