HCID 57893474, compound → HCID 57893562, compound

Participants

Reaction Steps

(3,4-Dichlorophenyl)(1H-pyrrolo[2,3-c]pyridin-2-yl)methanone (99 mg, 45%) was prepared as a yellow solid following the procedure described for Example 100 using (3,4-dichlorophenyl)(1H-pyrrolo[2,3-c]pyridin-2-yl)methanol (Example 113) and tetrahydrofuran as a solvent: mp 274-277° C. dec.; 1H NMR (500 MHz, DMSO-d6) δ7.24 (1H, s), 7.70 (1H, d, J=5.5 Hz), 7.87-7.95 (2H, m), 8.14 (1H, d, J=1.9 Hz), 8.22 (1H, d, J=5.6 Hz), 8.93 (1H, s), 12.50 (1H, s); ESI MS m/z 291 [C14H8Cl2N2O+H]+; HPLC (Method A) >99% (AUC), tR=17.4 min.

Provenance & Evidence