HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → HCID 10390732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | Pyrrole | HCID 8027 | — |
| Reactant | Pentapotassium Triphosphate | HCID 61695 | — |
| Reactant | HCID 18442679 | HCID 18442679 | — |
| Catalyst | Copper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI) | HCID 24350 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 10390732 | HCID 10390732 | — |
Reaction Steps
200 mg of 1,3-dichloro-5-(3,3-dichloro-allyloxy)-2-[3-(4-iodo-phenoxy)-propoxy]-benzene, 29 mg of pyrrole, 6.9 mg of copper(I) iodide, 2.2 mg of ethylenediamine and 155 mg of potassium triphosphate are stirred for 24 hours at 110° C. in 4 ml of dioxane. The reaction mixture is diluted with ethyl acetate and filtered. Concentration and purification over silica gel yield the title compound (compound 1.1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07608631B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-8e6e362e26fb42629792730ee4e22fd8 |
| Source note | uspto-grants-2009_10 |