HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Benzoyl-4-ethylphenol → 3-{4-[3-(2-Benzoyl-4-ethyl-phenoxy)-phenoxy]-2-methyl-phenyl}-propionic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Benzoyl-4-ethylphenol | HCID 13149653 | — |
| Reactant | 3-[4-(3-Bromo-phenoxy)-2-methyl-phenyl]-propionic acid methyl ester | HCID 57894192 | — |
| Product | 3-{4-[3-(2-Benzoyl-4-ethyl-phenoxy)-phenoxy]-2-methyl-phenyl}-propionic acid | HCID 11454455 | — |
Reaction Steps
The title compound is prepared by reacting the compound of 3-[4-(3-bromo-phenoxy)-2-methyl-phenyl]-propionic acid methyl ester with (5-ethyl-2-hydroxy-phenyl)-phenyl-methanone as in Example 18 to afford 0.220 g (50%). 1H NMR (400 MHz, CDCl3); HRMS (ES+) m/z exact mass calculated for C31H28O5 481.2015, found 481.2032 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07608639B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-024fe1fc878c4d65aa0b107947a9a4bb |
| Source note | uspto-grants-2009_10 |