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HRID1822275

反应详情

EQUATION

反应方程式

HRID 1822275 的结构方程式

REACTANTS

反应物

2
结构：Oc1ccc(Cl)cc1Oc1ccccc1
HCID12774295

4-Chloro-2-phenoxyphenol

C12H9ClO2

结构：COC(=O)CCc1ccc(Oc2ccc(Br)cc2)cc1C
HCID57894135

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Oc2ccc(Oc3ccc(Cl)cc3Oc3ccccc3)cc2)ccc1CCC(=O)O
HCID57894232

未命名化合物

PROCEDURE

实验过程

The title compound is prepared by reacting the compound of 3-[4-(4-bromo-phenoxy)-2-methyl-phenyl]-propionic acid methyl ester with 4-chloro-2-phenoxy-phenol as in Example 18 to afford 0.133 g (19%). 1H NMR (400 MHz, CDCl3); MS (ES−) m/z mass calculated for C28H23O5Cl 474, found 473 and 475 (M−1, and M+1, 100%).

WORKUP

后处理

  1. customto afford 0.133 g (19%)