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HRID1822445

反应详情

EQUATION

反应方程式

HRID 1822445 的结构方程式

REACTANTS

反应物

6
结构：NCC1CCCCC1
HCID76688

Cyclohexanemethylamine

C7H15N

结构：CC(C)(C)OC(=O)N[C@@H](Cc1ccccc1)C(=O)O
HCID77857

L-Phenylalanine, N-[(1,1-dimethylethoxy)carbonyl]-

C14H19NO4

结构：CC(C)(C)OC(=O)NC(C(=O)O)C(C)(C)C
HCID5046859

未命名化合物

结构：O=C([O-])NCl
HCID22035886

未命名化合物

结构：CC(C)(C)OC(=O)NC(C(=O)NC1c2ccccc2CC1O)C(C)(C)C
HCID68488177

未命名化合物

结构：C=CC1CC1(NC(=O)C1CC(Oc2cc(-c3ccccc3)nc3cc(OC)ccc23)CN1C(=O)NC(C(=O)NC1c2ccccc2CC1O)C(C)(C)C)C(=O)OCC
HCID68491628

未命名化合物

PRODUCTS

生成物

1
结构：C=C[C@@H]1C[C@]1(NC(=O)[C@@H]1C[C@@H](Oc2cc(-c3ccccc3)nc3cc(OC)ccc23)CN1C(=O)N[C@@H](Cc1ccccc1)C(=O)NCC1CCCCC1)C(=O)O
HCID68488115

未命名化合物

PROCEDURE

实验过程

N-(tert-butoxycarbonyl)-L-phenylalanine was attached to the resin as described for the preparation of compound 16 followed by reaction with cyclohexanemethylamine as described for the preparation of 17 and removal of the Boc group as described for 18. The afforded compound was then reacted with the chlorocarbamate achieved from 12 as described for the preparation of 13 which gave the title compound. Purity by HPLC>95%. M+H+760.4.