Acetic Acid → HCID 68490209, compound

Participants

Reaction Steps

Compound 128 (120 mg, 0.175 mmol) was dissolved in dioxane (9 ml) and water (6 ml). Lithium hydroxide (12 mg, 0.526 mmol) was added and the reaction was stirred at room temperature for 3.5 h. The mixture was acidified with acetic acid to pH=5, and co-evaporated with toluene. The crude product was used in the next step. MS (M+H+) 671

Provenance & Evidence