Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1822871Generated: October 31, 2026

HCID 10822192, compound → HCID 22170201, compound

https://huagongshe.com/reaction/1822871

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10822192HCID 10822192—
CatalystPalladiumHCID 23938—
SolventEthanol ethylacetateHCID 21584252—
ProductHCID 22170201HCID 2217020197.7%

Reaction Steps

A mixture of methyl 3-nitro-2-vinylbenzoate (1.1 g, 5.31 mmol), and 5% Pd/C (100 mg) in EtOAc/EtOH 1:1 (50 ml) was hydrogenated at 3 atm over night. The mixture was filtered through Celite, and the filtrate was concentrated to give the title compound 0.93 g (97%) as a colourless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07037925B2
Source datasetuspto-grants-2006_05
ORD IDord-70a7cb9a19d644eebe299f39c33200d8
Source noteuspto-grants-2006_05