HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorobenzaldehyde → (E)-1-Chloro-3-(2-(4-nitrophenyl)ethenyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorobenzaldehyde | HCID 11477 | — |
| Reactant | Diethyl 4-nitrobenzylphosphonate | HCID 256065 | — |
| Product | (E)-1-Chloro-3-(2-(4-nitrophenyl)ethenyl)benzene | HCID 6440392 | — |
Reaction Steps
In an analogous manner to that described in Example 36a), the reaction of diethyl (4-nitrobenzyl)phosphonate with 3-chlorobenzaldehyde yields the (E)-1-chloro-3-[2-(4-nitrophenyl)ethenyl]-benzene as an orange crystalline solid; MS: m/e=259 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07037935B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-967a2eb05a8045f98329dbac948d5c13 |
| Source note | uspto-grants-2006_05 |