2,3-Dichloro-5,6-dicyano-1,4-benzoquinone → HCID 22172341, compound

Participants

Reaction Conditions

Reaction Steps

The acetoxymethylacenaphthene (45 g) obtained in Step 3 was dissolved in dioxane (450 g). After the addition of dichlorodicyanobenzoquinone (60 g), the mixture was stirred for seven hours at 95° C. The reaction mixture was filtered and the solvent was evaporated from the filtrate to obtain 54 g of acetoxymethylacenaphthylene as a brown solid.

Provenance & Evidence