HCID 22147607, compound → HCID 22147619, compound

HRID 1823798Notes

Reaction equation

HRID 1823798 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:11]=[C:12]3[C:17]([C:18]([NH2:20])=[O:19])=[CH:16][CH:15]=[CH:14][N:13]3[CH:21]=2)=[CH:6][CH:5]=1)([O-])=O.[H][H]>[Pd]>[NH2:1][C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:11]=[C:12]3[C:17]([C:18]([NH2:20])=[O:19])=[CH:16][CH:15]=[CH:14][N:13]3[CH:21]=2)=[CH:6][CH:5]=1

Participants

4

Reactant 2

HCID 22147607HCID 22147607, compoundHCID 178418361HCID 178418361, compound

Product 1

HCID 22147619HCID 22147619, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

The product from Example 2 was dissolved in alcohol and, after addition of palladium/carbon, hydrogenated with hydrogen. This was followed by filtration and concentration of the filtrate in vacuo. The product was obtained.

Workup

  1. filtrationThis was followed by filtration and concentration of the filtrate in vacuo
  2. customThe product was obtained

Sources & evidence

ORD record
ord-ab5e3bec657d4f988eb306c055b8ff65
Source dataset
uspto-grants-2006_05
Patent number
US07041675B2

Reaction notes

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