HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Isocyanatomethylene)dibenzene → HCID 131725732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Isocyanatomethylene)dibenzene | HCID 4250935 | — |
| Reactant | Tropenol | HCID 53629842 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 131725732 | HCID 131725732 | — |
Reaction Steps
2.5 g (0.012 mol) of diphenylmethylisocyanate is placed in 7 mL acetonitrile, a solution of 1.67 g (0.012 mol) of tropenol in 5 mL acetonitrile is added dropwise. The solution is stirred for 24 hours at ambient temperature; after 10 minutes, a white precipitate is formed. After the end of the reaction time, the suspension is cooled and the precipitate is suction filtered. Yield: 2.28 g (55% of theory); melting point: 140° C.-142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07041674B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-edb6f2cc52174ca2b2dab547f2a297f5 |
| Source note | uspto-grants-2006_05 |