反应详情

Synthesis of this compound was achieved by the method set forth in Example 1, Part II above with the use of phenylacetylcyanamide in place of 4-methylbenzoylcyanamide and using 4-t-butylaniline hydrochloride instead of 4-isopropylaniline hydrochloride respectively. Yield 69%; m.p. 182–186° C.; Purity 86% (HPLC); 1H-NMR (CD3OD) δ 1.38 (s, 9H, CH3), 3.84 (s, 2H, CH2), 7.3 (d, 2H, ArH), 7.3–7.45 (m, 5H, ArH), 7.6 (d, 2H, ArH).

1. customSynthesis of this compound