HRID1824141

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11275335

8-Methoxy-3,4-dihydronaphthalen-1(2H)-one

C11H12O2

HCID18525171

4,5,6,7-Tetrahydro-1-benzofuran-4-amine

C8H11NO

PRODUCTS

生成物

HCID22147356

8-Methoxy-1,2,3,4-tetrahydronaphthalen-1-amine

C11H15NO

PROCEDURE

实验过程

Following the procedure for the preparation of 4,5,6,7-tetrahydro-1-benzofuran-4-amine but substituting 8-methoxy-3,4-dihydronaphthalen-1(2H)-one and making non-critical variations provided the title compound as a oil: 1H NMR (300 MHz, CDCl3) δ) 7.13, 6.73, 4.21, 3.87, 2.78–2.72, 1.88; HRMS (FAB) calcd for C11H15NO+H 178.1232, found 178.1232.