HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-Methoxy-3,4-dihydronaphthalen-1(2H)-one → 6-Methoxy-1-Indanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-Methoxy-3,4-dihydronaphthalen-1(2H)-one | HCID 11275335 | — |
| Reactant | 4,5,6,7-Tetrahydro-1-benzofuran-4-amine | HCID 18525171 | — |
| Product | 6-Methoxy-1-Indanamine | HCID 9920463 | — |
Reaction Steps
Following the procedure for the preparation of 4,5,6,7-tetrahydro-1-benzofuran-4-amine but substituting 8-methoxy-3,4-dihydronaphthalen-1(2H)-one and making non-critical variations provided the title compound as a oil: 1H NMR (CDCl3) δ 1.72, 2.54, 2.74, 2.90, 3.83, 4.34, 6.78, 6.91, 7.13; MS (FAB) m/z (rel. intensity) 164 (MH+, 17), 308 (8), 164 (17), 163 (7), 162 (19), 148 (18), 147 (99), 146 (18), 145 (9), 121 (11), 115 (8). HRMS (FAB) calcd for C10H13NO+H 164.1075, found 164.1071.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07041672B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-57f3f43e55024e2db6395c3e36055c1a |
| Source note | uspto-grants-2006_05 |