HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 2-Ethyl-6-methoxyindan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 6-Methoxy-alpha-tetralone | HCID 14112 | — |
| Reactant | 5-propyl-6,7-dihydro-1-benzothiophen-4(5H)-one | HCID 22147491 | — |
| Product | 2-Ethyl-6-methoxyindan-1-one | HCID 21840579 | — |
Reaction Steps
Following the procedure for the preparation of 5-propyl-6,7-dihydro-1-benzothiophen-4(5H)-one but substituting 6-methoxy 1-tetralone and ethyl iodide, and making non-critical variations provided the title compound as a oil: 1H NMR (CDCl3) δ 1.02, 1.55, 1.99, 2.68, 2.77, 3.27, 3.86, 7.21, 7.37; HRMS (FAB) calcd for C12H14O2+H 191.1072, found 191.1075.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07041672B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-9f3e55f60d584f1dbbc7c41c0e6a949f |
| Source note | uspto-grants-2006_05 |