HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(((Tert-butoxy)carbonyl)amino)butanoic acid → Methyl({2-[(tert-butoxycarbonyl)amino]butanoyl}amino)(cyclopropyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(((Tert-butoxy)carbonyl)amino)butanoic acid | HCID 333522 | — |
| Reactant | methyl{[N-(tert-butoxycarbonyl)-L-alanyl]amino}(cyclopropyl)acetate | HCID 58583288 | — |
| Product | Methyl({2-[(tert-butoxycarbonyl)amino]butanoyl}amino)(cyclopropyl)acetate | HCID 23593721 | — |
Reaction Steps
Following the procedure for the preparation of methyl{[N-(tert-butoxycarbonyl)-L-alanyl]amino}(cyclopropyl)acetate but substituting N-Boc-alpha-aminobutyric acid and making non-critical variations provided the title compound as a solid: 1H NMR (CDCl3) δ 0.40–0.62, 0.94–0.99, 1.09–1.12, 1.46, 1.63–2.06, 3.77, 4.04, 5.02, 6.54.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07041672B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-db1416645b4b42dea92408133286df18 |
| Source note | uspto-grants-2006_05 |