1,2-Difluoro-4-nitrobenzene → HCID 22148764, compound

HRID 1824346Notes

Reaction equation

HRID 1824346 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([N+:9]([O-:11])=[O:10])[CH:5]=[CH:6][C:7]=1F.[Cl:12][C:13]1[CH:14]=[C:15]([OH:19])[CH:16]=[N:17][CH:18]=1>>[F:1][C:2]1[CH:3]=[C:4]([N+:9]([O-:11])=[O:10])[CH:5]=[CH:6][C:7]=1[O:19][C:15]1[CH:14]=[C:13]([Cl:12])[CH:18]=[N:17][CH:16]=1

Participants

3

Reactant 2

HCID 1230531,2-Difluoro-4-nitrobenzeneHCID 5823053-Hydroxy-5-chloropyridine

Product 1

HCID 22148764HCID 22148764, compound

Procedure

3,4-Difluoronitrobenzene (5.0 g, 32 mmol) and 5-chloro-3-pyridinol were combined using the procedure described in Example 1, to produce 8.2 g of the title compound.

Sources & evidence

ORD record
ord-374cdc3be67f4d609d7dde9778f84568
Source dataset
uspto-grants-2006_05
Patent number
US07041691B1

Reaction notes

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