HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloronitrobenzene → HCID 22148843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloronitrobenzene | HCID 11899 | — |
| Reactant | 3-Hydroxy-5-chloropyridine | HCID 582305 | — |
| Product | HCID 22148843 | HCID 22148843 | — |
Reaction Steps
5-Chloro-3-pyridinol (5 g, Aldrich) and 2,4-dichloronitrobenzene (7.4 g, Aldrich) were combined as described in Example 1. The title compound was isolated as the minor product using gravity chromatography on silica eluting with 10% ethyl acetate/hexanes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07041691B1 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-fd0ea225510b43beb989c45a4c8a2e65 |
| Source note | uspto-grants-2006_05 |