2-Naphthalenethiol → HCID 22148887, compound

HRID 1824353Notes

Reaction equation

HRID 1824353 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N+:9]([O-:11])=[O:10])[CH:5]=[CH:6][C:7]=1F.[CH:12]1[C:21]2[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=2)[CH:15]=[CH:14][C:13]=1[SH:22]>>[Cl:1][C:2]1[CH:3]=[C:4]([N+:9]([O-:11])=[O:10])[CH:5]=[CH:6][C:7]=1[S:22][C:13]1[CH:14]=[CH:15][C:16]2[C:21](=[CH:20][CH:19]=[CH:18][CH:17]=2)[CH:12]=1

Participants

3

Reactant 2

HCID 70582-NaphthalenethiolHCID 676882-Chloro-1-fluoro-4-nitrobenzene

Product 1

HCID 22148887HCID 22148887, compound

Procedure

2-(2-Chloro-4-nitro-phenylsulfanyl)-napthalene was synthesized (100%) from 3-chloro-4-fluoro-nitrobenzene (Aldrich) and napthalene-2-thiol (Avocado) in a similar manner as described in example 89.

Sources & evidence

ORD record
ord-bc050e0af3cb4465b1b20272edc1bbd0
Source dataset
uspto-grants-2006_05
Patent number
US07041691B1

Reaction notes

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