2-Chloro-1-fluoro-4-nitrobenzene → HCID 22148775, compound

HRID 1824381Notes

Reaction equation

HRID 1824381 reaction equation
[SH:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][C:8]([C:11]([OH:13])=[O:12])=[CH:7][C:5]=2[N:6]=1.[Cl:14][C:15]1[CH:20]=[C:19]([N+:21]([O-:23])=[O:22])[CH:18]=[CH:17][C:16]=1F>>[Cl:14][C:15]1[CH:20]=[C:19]([N+:21]([O-:23])=[O:22])[CH:18]=[CH:17][C:16]=1[S:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][C:8]([C:11]([OH:13])=[O:12])=[CH:7][C:5]=2[N:6]=1

Participants

3

Reactant 2

HCID 676882-Chloro-1-fluoro-4-nitrobenzeneHCID 178524192HCID 178524192, compound

Product 1

HCID 22148775HCID 22148775, compound

Procedure

2-(2-chloro-4-nitro-phenylsulfanyl)-benzothiazol-5-carboxylic acid was prepared (66%) from 2-mercapto-benzothiazol-5-carboxylic acid (240) and 2-chloro-1-fluoro-4-nitrobenzene, obtained from Aldrich, in a similar manner as described in example 251.

Sources & evidence

ORD record
ord-98f3a0b5854c4a1cbb8b6e475e3f24b8
Source dataset
uspto-grants-2006_05
Patent number
US07041691B1

Reaction notes

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