Benzylamine → HCID 178478324, compound

HRID 1824456Notes

Reaction equation

HRID 1824456 reaction equation
[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([NH:6][CH:7]=[N:8]2)=[C:4](Cl)[N:3]=1.[CH2:12]([NH2:19])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>C(O)CCC>[Cl:1][C:2]1[NH:3][C:4]([NH:19][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:5]2[C:9]([N:10]=1)=[N:8][CH:7]=[N:6]2

Participants

4

Reactant 2

HCID 7504BenzylamineHCID 53244122,6-Dichloropurine

Product 1

HCID 178478324HCID 178478324, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Conditions

Temperature
75 °C

Procedure

189 mg of 2,6-dichloropurine, 4 ml of butanol and 0.12 ml (1.1 mol) of benzylarnine are mixed at room temperature and the medium is heated at a temperature of 75° C. for 5 hours and then it is left at room temperature overnight.

Sources & evidence

ORD record
ord-54285df284bd4696a87b5b6538351ffd
Source dataset
uspto-grants-2006_05
Patent number
US07041824B2

Reaction notes

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