P-Anisidine → HCID 178492213, compound

HRID 1824457Notes

Reaction equation

HRID 1824457 reaction equation
[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([NH:6][CH:7]=[N:8]2)=[C:4](Cl)[N:3]=1.[CH3:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([NH2:20])=[CH:16][CH:15]=1>C(O)CCC>[Cl:1][C:2]1[NH:3][C:4]([NH:20][C:17]2[CH:18]=[CH:19][C:14]([O:13][CH3:12])=[CH:15][CH:16]=2)=[C:5]2[C:9]([N:10]=1)=[N:8][CH:7]=[N:6]2

Participants

4

Reactant 2

HCID 7732P-AnisidineHCID 53244122,6-Dichloropurine

Product 1

HCID 178492213HCID 178492213, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Conditions

Temperature
75 °C

Procedure

189 mg of 2,6-dichloropurine, 4 ml of butanol and 135 mg (1.1 mol) of 4-methoxybenzenamine are mixed at room temperature and the medium is heated at a temperature of 75° C. for 5 hours and then left at room temperature overnight.

Sources & evidence

ORD record
ord-f6d2580f37d5413cab92438dbcabba0b
Source dataset
uspto-grants-2006_05
Patent number
US07041824B2

Reaction notes

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