4-Chloroaniline → HCID 178478206, compound

HRID 1824461Notes

Reaction equation

HRID 1824461 reaction equation
[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([NH:6][CH:7]=[N:8]2)=[C:4](Cl)[N:3]=1.[Cl:12][C:13]1[CH:19]=[CH:18][C:16]([NH2:17])=[CH:15][CH:14]=1>C(O)CCC>[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][NH:8]2)=[C:4]([NH:17][C:16]2[CH:18]=[CH:19][C:13]([Cl:12])=[CH:14][CH:15]=2)[N:3]=1

Participants

4

Reactant 2

HCID 78124-ChloroanilineHCID 53244122,6-Dichloropurine

Product 1

HCID 178478206HCID 178478206, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

The procedure is carried out as in Example 1, starting with 472.5 mg of 2,6-dichloropurine, 5 ml of butanol and 398.0 mg of para-chloroaniline. 700.3 mg of the expected product are thus obtained.

Sources & evidence

ORD record
ord-6654c6b5e8694e70a602366e44d391b1
Source dataset
uspto-grants-2006_05
Patent number
US07041824B2

Reaction notes

Loading…