HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → 6,7-dihydro-8(5H)-quinolinone oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | 6,7-Dihydro-5H-quinoline-8-one | HCID 11744777 | — |
| Product | 6,7-dihydro-8(5H)-quinolinone oxime | HCID 135742185 | 96% |
Reaction Steps
According to the reported procedure (J. Het. Chem. 1978, 15, 249-251), 6,7-dihydro-5H-quinolin-8-one was reacted with hydroxylamine hydrochloride to afford the title compound (2.40 g, 96%) as a white solid after drying in vacuo: MS (ES) m/e 163 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07741339B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-1382ae0096284cf9bc5ffb77632a706b |
| Source note | uspto-grants-2010_06 |