Methanesulfonamide → HCID 69316356, compound

HRID 1824863Notes

Reaction equation

HRID 1824863 reaction equation
[C:1]1([C:7]2[CH2:16][CH2:15][C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[C:8]=2[C:17]2[CH:22]=[CH:21][C:20]([CH:23]=[CH:24][C:25]([OH:27])=O)=[CH:19][CH:18]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:28][S:29]([NH2:32])(=[O:31])=[O:30]>>[C:1]1([C:7]2[CH2:16][CH2:15][C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[C:8]=2[C:17]2[CH:22]=[CH:21][C:20]([CH:23]=[CH:24][C:25]([NH:32][S:29]([CH3:28])(=[O:31])=[O:30])=[O:27])=[CH:19][CH:18]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 72879MethanesulfonamideHCID 69317421HCID 69317421, compound

Product 1

HCID 69316356HCID 69316356, compound

Procedure

Prepared by coupling 2m and methylsulfonamide in accordance with Procedure 1, Method A described hereinabove. Yield (57%); ESI m/z: 428 (M−H−, 100%).

Workup

  1. customPrepared
  2. customYield (57%)

Sources & evidence

ORD record
ord-3870d0789ec240058ec6cf08b66964c1
Source dataset
uspto-grants-2006_05
Patent number
US07045540B2

Reaction notes

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