Benzenesulfonamide → HCID 69780746, compound

HRID 1824867Notes

Reaction equation

[C:1]1([C:7]2[CH2:8][O:9][C:10]3[C:15]([C:16]=2[C:17]2[CH:22]=[CH:21][C:20]([CH:23]=[CH:24][C:25](O)=[O:26])=[CH:19][CH:18]=2)=[CH:14][CH:13]=[CH:12][CH:11]=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:28]1([S:34]([NH2:37])(=[O:36])=[O:35])[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1>>[C:1]1([C:7]2[CH2:8][O:9][C:10]3[C:15]([C:16]=2[C:17]2[CH:18]=[CH:19][C:20]([CH:23]=[CH:24][C:25]([NH:37][S:34]([C:28]4[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=4)(=[O:36])=[O:35])=[O:26])=[CH:21][CH:22]=2)=[CH:14][CH:13]=[CH:12][CH:11]=3)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

Reactant 2

HCID 7370Benzenesulfonamide

HCID 69317447HCID 69317447, compound

Product 1

HCID 69780746HCID 69780746, compound

Procedure

Prepared by coupling 3d and benzene sulfonamide in accordance with Procedure 1, Method A described hereinabove. Yield (46%); ESI m/z: 492 (M−H−, 100%).

Workup

customPrepared
customYield (46%)

Sources & evidence

ORD record: ord-5b988d98eb89482b8065987ffaa7e675
Source dataset: uspto-grants-2006_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07045540B2

Reaction notes

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