HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[4-(Z)-(1,2-diphenylbut-1-enyl)phenyl]-acrylic acid → N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-3-methoxy-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[4-(Z)-(1,2-diphenylbut-1-enyl)phenyl]-acrylic acid | HCID 3036152 | — |
| Reactant | 3-Methoxybenzene-1-sulfonamide | HCID 14763060 | — |
| Product | N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-3-methoxy-benzenesulfonamide | HCID 69780580 | — |
Reaction Steps
Prepared by coupling 1a and 3-methoxybenzenesulfonamide (Synlett, 1997, 375) in accordance with Procedure 1, Method B described hereinabove. Yield (27%); 1H NMR (d6-DMSO) δ 12.18 (br s, 1H), 7.53–7.07 (m, 17H), 6.84 (d, J=8.0 Hz, 2H), 6.40 (d, J=15.7 Hz, 1H), 3.78 (s, 3H), 2.35 (q, J=7.4 Hz, 2H), 0.82 (t, J=7.4 Hz, 3H); APcI m/z: 522 (M−H−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07045540B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-19fce159a4b84d4991f46bea11e81739 |
| Source note | uspto-grants-2006_05 |