HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanesulfonamide → HCID 86760605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanesulfonamide | HCID 73702 | — |
| Reactant | 3-[4-(Z)-(1,2-diphenylbut-1-enyl)phenyl]-acrylic acid | HCID 3036152 | — |
| Product | HCID 86760605 | HCID 86760605 | — |
Reaction Steps
Prepared by coupling 1a and ethanesulfonamide (Synlett, 1997, 375) in accordance with Procedure 1, Method B described hereinabove. Yield (25%); 1H NMR (d6-DMSO) δ 11.67 (br s, 1H), 7.47 (d, J=15.7 Hz, 1H), 7.40–7.09 (m, 12H), 6.86 (d, J=8.4 Hz, 2H), 6.47 (d, J=15.7 Hz, 1H), 3.37 (q, J=7.4 Hz, 2H), 2.36 (q, J=7.3 Hz, 2H), 1.16 (t, J=7.3 Hz, 3H), 0.83 (t, J=7.3 Hz, 3H); APcI m/z: 444 (M−H−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07045540B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-191912d143a84c05bc7ccf170178e5d2 |
| Source note | uspto-grants-2006_05 |