HCID 69780647, compound → HCID 54486062, compound

HRID 1824902Notes

Reaction equation

HRID 1824902 reaction equation
C[O:2][C:3](=[O:30])[CH:4]=[CH:5][C:6]1[CH:11]=[CH:10][C:9]([CH:12]2[C:21]3[C:16](=[CH:17][C:18]([O:22][CH3:23])=[CH:19][CH:20]=3)[CH2:15][CH2:14][CH:13]2[C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)=[CH:8][CH:7]=1>CC#N>[CH3:23][O:22][C:18]1[CH:17]=[C:16]2[C:21](=[CH:20][CH:19]=1)[CH:12]([C:9]1[CH:10]=[CH:11][C:6]([CH:5]=[CH:4][C:3]([OH:30])=[O:2])=[CH:7][CH:8]=1)[CH:13]([C:24]1[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=1)[CH2:14][CH2:15]2

Participants

3

Reactant 1

HCID 69780647HCID 69780647, compound

Product 1

HCID 54486062HCID 54486062, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

Prepared by saponifying (hydrolyzing) ester 6d in accordance with the general method described in Example VII. Yield (93%); APcI m/z: 426 (M+H+CH3CN+, 100%).

Workup

  1. customPrepared
  2. customYield (93%)

Sources & evidence

ORD record
ord-ab23dd8caa654f36b69813a71dc4ce87
Source dataset
uspto-grants-2006_05
Patent number
US07045540B2

Reaction notes

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