HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 22144913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 22144936 | HCID 22144936 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22144913 | HCID 22144913 | 90% |
Reaction Steps
Beginning with 3.5 gm (15 mMol) 2-allyl-4-fluoro-5-bromophenol, the title compound was prepared in 90% yield essentially by the procedure described in Preparation XXXI with the exception that the cyclization/dehydration step was performed using sulfuric acid in toluene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07045545B1 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-8c7aafa419f44e708b57a192955d5aff |
| Source note | uspto-grants-2006_05 |