HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → 2-(5-Fluorobenzofur-7-yl)-1-aminoethane oxalate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | Borane | HCID 6331 | — |
| Reactant | 2-(5-Fluorobenzofur-7-yl)propionamide | HCID 22144813 | — |
| Reactant | 2-(5-Fluorobenzofur-7-yl)-1-aminoethane | HCID 22144824 | — |
| Product | 2-(5-Fluorobenzofur-7-yl)-1-aminoethane oxalate | HCID 22144823 | — |
Reaction Steps
Beginning with 2-(5-fluorobenzofur-7-yl)propionamide (EXAMPLE 39), 2-(5-fluorobenzofur-7-yl)-1-aminoethane was prepared by borane reduction essentially as described in EXAMPLE 39. This amine was treated with oxalic acid to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07045545B1 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-6703aca2bc084158a42f0794f70967b6 |
| Source note | uspto-grants-2006_05 |