HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Bromo-1-(4-ethylphenyl)ethan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4'-Ethylacetophenone | HCID 13642 | — |
| Reactant | Bromine | HCID 24408 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-Bromo-1-(4-ethylphenyl)ethan-1-one | HCID 12401951 | — |
Reaction Steps
20 mmol of 1-(4-ethylphenyl)ethan-1-one, 1 ml conc. HCl were mixed in 20 ml diethyl ether at 0° C. under nitrogen. To this solution a solution of 20 mmol Br2 in 20 ml chloroform was added drop wise and left for four hours and then concentrated in vacuo to obtain 2-bromo-1-(4-ethylphenyl)ethan-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07045519B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-d84570eeeb684c5bb40cacc334df1433 |
| Source note | uspto-grants-2006_05 |