HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69637166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-[(3-Oxo-3,4-dihydro-2H-1,4-benzoxazin-2-ylidene)methyl]phenyl acetate | HCID 57224333 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 69637166 | HCID 69637166 | — |
Reaction Steps
A mixture of 2-[(4-acetoxyphenyl)methylene]-2H-1,4-benzoxazin-3(4H)-one (0.49 g, 0.0016 mol) and NaOH 10% (30 ml) was refluxed for 1 h. The reaction mixture was cooled and acidified with 6N HCl. The precipitated was collected by filtration, then washed with water and dried. The crude product was purified by recrystalization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07049312B1 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-ec8bef30b1414ab1980787041818e997 |
| Source note | uspto-grants-2006_05 |