HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 3006092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Benzoin | HCID 8400 | — |
| Reactant | (3-Chlorophenyl)hydrazine | HCID 75332 | — |
| Reactant | Potassium thiocyanate | HCID 516872 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 3006092 | HCID 3006092 | 56% |
Reaction Steps
A mixture of benzoine (1.0 g, 0.0071 mol), KSCN (0.68 g, 0.0071 mol) and 3-chlorophenylhydrazine×HCl (1.26 g, 0.0071 mol) was stirred in acetic acid (10 mL) for two days. The white precipitate formed was filtered off (0.4 g). Water (50 mL) was added and the precipitate formed was filtered off. Recrystallization from MeOH/water (1:1) yielded 1.5 g (56%) of 9.26.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07049332B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-ba9d8137f63144429ee8913a1f5f85ed |
| Source note | uspto-grants-2006_05 |