HRID1826516

反应详情

EQUATION

反应方程式

HRID 1826516 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A suspension of 2-(2 (S)-amino-3-phenyl-propylamino)-3-methyl-5-nitro-6-pyridin-4-yl-3H-pyrimidin-4-one (0.2 mmol) and Pd/C was stirred over a hydrogen filled balloon for 1 h at room temperature. The product was filtered through a bed of celite, and the solvents removed under vacuum. The product was purified on reverse phase HPLC M+1=351.

WORKUP

后处理

  1. filtrationThe product was filtered through a bed of celite
  2. customthe solvents removed under vacuum
  3. customThe product was purified on reverse phase HPLC M+1=351